Cooling Mixtures
Assembling Apparatus
Chromatography
Cooling
Cooling Mixtures
Dean-Stark Apparatus
Distillation
Drying Liquids
Filtration
Heating
IR Spectroscopy
Measuring Melting Points
Recrystallisation
Reflux
Rotary Evaporation
Solvent Extraction
Soxhlet Extraction
Volumetric Analysis
Weighing

 

Coolant Temperature Comments
Ice Bath
0 - 5 o C
 It is important to have a crushed ice - water mixture to ensure good conduction.
Crushed Ice - CaCl2.6H2O (2.5:1)
-10 o C 
These baths are 'dry' mixtures and so conduction of heat away from a vessel wiill be inefficient.
Crushed Ice - NaCl (3:1)
-20 o C 
Crushed Ice - CaCl2.6H2O (0.8:1)
-40 o C 
Dry Ice - Acetone (propanone)
 -78o C 
Dry ice can cause severe frostbite if it comes in contact with bare skin so insulating gloves sould always be worn. The baths should be made up with small pieces of the solid and topped up with further dry ice periodically.
Liquid Nitrogen
 -196o C  
Liquid Nitrogen is a hazardous material that can cause severe frostbite in contact with bare skin so insulating gloves should always be worn. Because of the risk of suffocation liquid nitrogen should only be used in well ventillated areas.