Measuring Melting Points
Assembling Apparatus
Chromatography
Cooling
Dean-Stark Apparatus
Distillation
Drying Liquids
Filtration
Heating
IR Spectroscopy
Measuring Melting Points
Apparatus Guide
Video Instructions
Recrystallisation
Reflux
Rotary Evaporation
Solvent Extraction
Soxhlet Extraction
Volumetric Analysis
Weighing

The measurement of melting points is a relatively straightforward procedure that is carried out to determine the purity of a compound or to assist with its identification. A pure compound will melt over a relatively narrow temperature range, impurities both lowering temperature and widening the range over which it melts. The apparatus used to measure melting points can be simple oil baths to 'hot-stage' apparatus where the melting process is observed with the aid of a microscope. In each case the range of temperatures a compound melts is recorded and compared with known data.

Melting point apparatus (detail)